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Intracellular Staining

introduction

Flow cytometry is a powerful tool for analyzing cell populations based on surface and intracellular markers. Intracellular staining allows for the detection of molecules within cells, including intracellular biomarkers. Some of the intracellular biomarkers that can be examined include:

Cytokines such as IFN-γ, TNF-α, IL-2

Transcription factors (e.g., FoxP3, STAT proteins)

Signaling molecules (e.g., phosphoproteins like pERK, pAkt)

Intracellular proteins, for example, Ki-67 for proliferation and Bcl-2 for apoptosis.

Key Steps in Intracellular Staining

Cell Stimulation for Activation of Cytokine-Related Signaling Pathways

To detect cytokines, cells are often stimulated with agents like PMA/Ionomycin or specific antigens.

Protein transport inhibitors (e.g., Brefeldin A, Monensin) prevent cytokine secretion, allowing accumulation inside the cell.

Surface Staining

Before fixation and permeabilization, surface markers (e.g., CD4, CD8) can be stained to identify cell subsets.

Fixation

Cells are fixed using formaldehyde or paraformaldehyde (PFA) to preserve cellular structure and immobilize proteins.

Permeabilization

Detergent-based buffers (e.g., saponin, Triton X-100) create pores in the membrane, allowing antibodies to access intracellular targets.

Methanol permeability may be used for nuclear targets, such as FoxP3 and Ki-67.

Intracellular Staining

Cells are incubated with fluorescently labeled antibodies against the target molecule.

Isotype controls and fluorescence minus one (FMO) controls are essential for accurate interpretation.

Applications

  1. Immunology: Profiling cytokines in Th1/Th2/Th17 cells

  2. Cancer Research: Detection of phosphorylated signaling proteins

  3. Stem Cell Studies: Analysis of transcription factors such as Oct4 and Nanog.